Sell Vitamin C powder (Ascorbic Acid)

Description

REQUIREMENTS
Identification
A. A 1: *0 aqueous solution slowly reduces alkaline cupric tartrate TS at *5 C but more readily upon heating.
B. The infrared absorption spectrum of a potassium bromide dispersion of the sample exhibits maxima at the same wavelengths as those of a similar preparation of USP Ascorbic Acid Reference Standard.
Assay Not less than *9.0% and not more than **0.5% of C6H8O6.
Lead Not more than 2 mg/kg.
Optical (Specific) Rotation D*5: Between **0.5and **1.5.
Residue on Ignition Not more than 0.1%.

TESTS
Assay Dissolve about **0 mg of sample, accurately weighed, in a mixture of **0 mL of water, recently boiled and cooled, and *5 mL of 2 N sulfuric acid. Titrate the solution immediately with 0.1 N iodine, adding starch TS near the endpoint. Each milliliter of 0.1 N iodine is equivalent to 8.**6 mg of C6H8O6.
Lead Determine as directed in the Flame Atomic Absorption Spectrophotometric Method under Lead Limit Test, Appendix IIIB, using a **-g sample.
Optical (Specific) Rotation Determine as directed under Optical (Specific) Rotation, Appendix IIB, using a solution containing 1 g of sample in *0 mL of carbon dioxide-free water.
Residue on Ignition Determine as directed under Residue on Ignition, Appendix IIC, igniting a *-g sample.
Packaging and Storage Store in tight, light-resistant containers